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Crystal Structure of 4,4′-Diphenyl-2,2′-dithioxo-[4,4′-biimidazolidine]-5,5′-dione Bis(dimethylsulfoxide) Solvate
http://hdl.handle.net/2297/28463
http://hdl.handle.net/2297/284639cb3a445-c99d-4bca-92f5-d9b51e49574d
名前 / ファイル | ライセンス | アクション |
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TE-PR-KUNIMOTO-K-201.pdf (130.6 kB)
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Item type | 学術雑誌論文 / Journal Article(1) | |||||
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公開日 | 2017-10-03 | |||||
タイトル | ||||||
タイトル | Crystal Structure of 4,4′-Diphenyl-2,2′-dithioxo-[4,4′-biimidazolidine]-5,5′-dione Bis(dimethylsulfoxide) Solvate | |||||
言語 | ||||||
言語 | eng | |||||
資源タイプ | ||||||
資源タイプ識別子 | http://purl.org/coar/resource_type/c_6501 | |||||
資源タイプ | journal article | |||||
著者 |
Ogawa, Toshikazu
× Ogawa, Toshikazu× Kitoh, Sohichi× Ogawa, Masaaki× Ichitani, Masaki× Kuwae, Akio× Hanai, Kazuhiko× Kunimoto, Koki |
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書誌情報 |
Analytical Sciences: X-ray Structure Analysis Online 巻 23, p. x201-x202, 発行日 2007-01-01 |
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ISSN | ||||||
収録物識別子タイプ | ISSN | |||||
収録物識別子 | 1348-2238 | |||||
DOI | ||||||
関連タイプ | isIdenticalTo | |||||
識別子タイプ | DOI | |||||
関連識別子 | 10.2116/analscix.23.x201 | |||||
出版者 | ||||||
出版者 | 日本分析化学会 = The Japan Society for Analytical Chemistry | |||||
抄録 | ||||||
内容記述タイプ | Abstract | |||||
内容記述 | The crystal structure of the 1:2 dimethylsulfoxide solvate of 4,4′-diphenyl-2,2′-dithioxo-[4,4′-biimidazolidine]-5,5′-dione(I) has been determined by X-ray diffraction. The crystal belongs to space group C2/c with cell dimensions of a = 23.81(1)Å, b = 9.884(5)Å, c = 12.536(8)Å, β = 117.38(1)°. The compound, C18H14N4O2S2·2C2H6OS, crystallizes with half a molecule in the asymmetric unit, the molecule being centrosymmetric. The centre of inversion lies on the middle of the C(3)-C(3)′ bond. In crystals, the molecules form two N-H…O cyclic hydrogen bonds in a cyclic R22(12) arrangement, each of which forms on either side. DMSO molecules are hydrogen-bonded to the amide N-H groups. This hydrogen bond network forms an infinite tape structure along the c-axis. | |||||
権利 | ||||||
権利情報 | Copyright (c) 2007 by The Japan Society for Analytical Chemistry | |||||
著者版フラグ | ||||||
出版タイプ | VoR | |||||
出版タイプResource | http://purl.org/coar/version/c_970fb48d4fbd8a85 | |||||
関連URI | ||||||
識別子タイプ | URI | |||||
関連識別子 | https://japanlinkcenter.org/JST.JSTAGE/analscix/23.x201 | |||||
関連URI | ||||||
識別子タイプ | URI | |||||
関連識別子 | http://wwwsoc.nii.ac.jp/jsac/ |