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A new synthetic method for dipeptides containing α,β- didehydroamino acids utilizing an α-tosylglycine residue
http://hdl.handle.net/2297/38279
http://hdl.handle.net/2297/38279f054f3e7-b2bc-4d74-aa50-f9995f21eb11
| 名前 / ファイル | ライセンス | アクション |
|---|---|---|
SC-PR-KIOSHITA-H-2219.pdf (165.6 kB)
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| Item type | 学術雑誌論文 / Journal Article(1) | |||||
|---|---|---|---|---|---|---|
| 公開日 | 2017-10-03 | |||||
| タイトル | ||||||
| タイトル | A new synthetic method for dipeptides containing α,β- didehydroamino acids utilizing an α-tosylglycine residue | |||||
| 言語 | ||||||
| 言語 | eng | |||||
| 資源タイプ | ||||||
| 資源タイプ識別子 | http://purl.org/coar/resource_type/c_6501 | |||||
| 資源タイプ | journal article | |||||
| 著者 |
Shiraishi, Yohsuke
× Shiraishi, Yohsuke× Yamauchi, Hiroshi× Takamura, Takashi× Kinoshita, Hideki |
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| 書誌情報 |
Bulletin of the Chemical Society of Japan 巻 77, 号 12, p. 2219-2229, 発行日 2004-01-01 |
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| ISSN | ||||||
| 収録物識別子タイプ | ISSN | |||||
| 収録物識別子 | 0009-2673 | |||||
| NCID | ||||||
| 収録物識別子タイプ | NCID | |||||
| 収録物識別子 | AA00580132 | |||||
| DOI | ||||||
| 関連タイプ | isIdenticalTo | |||||
| 識別子タイプ | DOI | |||||
| 関連識別子 | 10.1246/bcsj.77.2219 | |||||
| 出版者 | ||||||
| 出版者 | The Chemical Society of Japan = 日本化学会 | |||||
| 抄録 | ||||||
| 内容記述タイプ | Abstract | |||||
| 内容記述 | The reaction of peptides containing an N-Boc- or N-Z-α-tosylglycine residue at the N-terminus with a variety of excess nitro compounds under basic conditions to give the nitro compound-adducts in good yields, followed by the elimination of nitrous acid from the adducts to afford the corresponding dipeptide containing α,β-didehydroamino acids with (Z)-configuration predominantly. Treatment of the same starting materials with aldehydes in the presence of base and tributylphosphine also gave a dipeptide containing α,β-didehydroamino acids with high (Z)-selectivity in satisfactory yields. The present method can be successfully applied to the synthesis of a protected leucine enkephalin analog. | |||||
| 権利 | ||||||
| 権利情報 | Copyright © The Chemical Society of Japan 日本化学会 | |||||
| 著者版フラグ | ||||||
| 出版タイプ | VoR | |||||
| 出版タイプResource | http://purl.org/coar/version/c_970fb48d4fbd8a85 | |||||
| 関連URI | ||||||
| 識別子タイプ | URI | |||||
| 関連識別子 | https://www.jstage.jst.go.jp/browse/bcsj | |||||
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| 識別子タイプ | URI | |||||
| 関連識別子 | http://www.chemistry.or.jp/ | |||||
