{"created":"2023-07-27T06:51:58.337970+00:00","id":45618,"links":{},"metadata":{"_buckets":{"deposit":"3eca22cf-898f-40bd-9bf7-4b3dd7a344dd"},"_deposit":{"created_by":18,"id":"45618","owners":[18],"pid":{"revision_id":0,"type":"depid","value":"45618"},"status":"published"},"_oai":{"id":"oai:kanazawa-u.repo.nii.ac.jp:00045618","sets":["2812:2813:2820"]},"author_link":["50470","79246"],"item_9_biblio_info_8":{"attribute_name":"書誌情報","attribute_value_mlt":[{"bibliographicIssueDates":{"bibliographicIssueDate":"2014-06-03","bibliographicIssueDateType":"Issued"},"bibliographicPageStart":"4p.","bibliographicVolumeNumber":"2012-04-01 - 2014-03-31","bibliographic_titles":[{"bibliographic_title":"平成25(2013)年度 科学研究費補助金 若手研究(B) 研究成果報告書"},{"bibliographic_title":"2013 Fiscal Year Final Research Report","bibliographic_titleLang":"en"}]}]},"item_9_creator_33":{"attribute_name":"著者別表示","attribute_type":"creator","attribute_value_mlt":[{"creatorNames":[{}],"nameIdentifiers":[{},{},{}]}]},"item_9_description_21":{"attribute_name":"抄録","attribute_value_mlt":[{"subitem_description":"本研究では、固体２次元交換核磁気共鳴測定を用いてアミノ酸の固体粉末試料の炭素核距離を解析した。試料には２つの炭素原子核を炭素１３で標識したアミノ酸（ロイシン, アラニン）を用いた。解析の結果、アラニンのメチン基とメチル基の炭素核間距離（文献値は１．５３Å）は０．９～１．６Åと見積もることができた。また、ロイシンのメチン基とカルボキシ基の炭素核間距離（文献値は１．５３Å）は１．６Å以下と見積もられたが、距離の範囲の下限を見積もることはできなかった。以上より、本手法は水素核が直接結合した炭素同士であれば、距離の範囲を見積もることができる可能性が示唆された。","subitem_description_type":"Abstract"},{"subitem_description":"In this study, the distances between two carbon nuclei in amino acids were estimated from time-dependence of signals recorded by measurements of two-dimensional exchange solid-state nuclear magnetic resonance. We analyzed two amino acids (l-Leucine, l-Alanine) which were labeled two carbon nuclei with carbon-13. We succeeded to estimate the distance between the two carbons of methine and methyl groups in l-Alanine from 0.9 to 1.6 angstroms. Although it was estimated that the distance between carbon nuclei of methine and carboxyl groups in l-Leucine was less than 1.6 angstroms, we could not estimate the lower limit of the distance of l-Leucine. From the above, it is indicated that ranges of distances among carbon nuclei directly-bonding hydrogen nuclei are possibly estimated.","subitem_description_type":"Abstract"}]},"item_9_description_22":{"attribute_name":"内容記述","attribute_value_mlt":[{"subitem_description":"研究課題/領域番号:24750014, 研究期間(年度):2012-04-01 - 2014-03-31","subitem_description_type":"Other"},{"subitem_description":"出典：研究課題「固体NMRによる結晶化が困難なタンパク質のための構造解析法の開発」課題番号24750014\n（KAKEN：科学研究費助成事業データベース（国立情報学研究所））\n（https://kaken.nii.ac.jp/report/KAKENHI-PROJECT-24750014/24750014seika/）を加工して作成","subitem_description_type":"Other"}]},"item_9_identifier_registration":{"attribute_name":"ID登録","attribute_value_mlt":[{"subitem_identifier_reg_text":"10.24517/00051955","subitem_identifier_reg_type":"JaLC"}]},"item_9_publisher_17":{"attribute_name":"公開者","attribute_value_mlt":[{"subitem_publisher":"金沢大学理工研究域物質化学系"}]},"item_9_relation_28":{"attribute_name":"関連URI","attribute_value_mlt":[{"subitem_relation_name":[{"subitem_relation_name_text":"https://kaken.nii.ac.jp/search/?qm=50533577"}],"subitem_relation_type_id":{"subitem_relation_type_id_text":"https://kaken.nii.ac.jp/search/?qm=50533577","subitem_relation_type_select":"URI"}},{"subitem_relation_name":[{"subitem_relation_name_text":"https://kaken.nii.ac.jp/grant/KAKENHI-PROJECT-24750014/"}],"subitem_relation_type_id":{"subitem_relation_type_id_text":"https://kaken.nii.ac.jp/grant/KAKENHI-PROJECT-24750014/","subitem_relation_type_select":"URI"}},{"subitem_relation_name":[{"subitem_relation_name_text":"https://kaken.nii.ac.jp/report/KAKENHI-PROJECT-24750014/24750014seika/"}],"subitem_relation_type_id":{"subitem_relation_type_id_text":"https://kaken.nii.ac.jp/report/KAKENHI-PROJECT-24750014/24750014seika/","subitem_relation_type_select":"URI"}}]},"item_9_version_type_25":{"attribute_name":"著者版フラグ","attribute_value_mlt":[{"subitem_version_resource":"http://purl.org/coar/version/c_ab4af688f83e57aa","subitem_version_type":"AM"}]},"item_files":{"attribute_name":"ファイル情報","attribute_type":"file","attribute_value_mlt":[{"accessrole":"open_date","date":[{"dateType":"Available","dateValue":"2018-08-23"}],"displaytype":"detail","filename":"SC-PR-OHASHI-R-kaken 2014-4p.pdf","filesize":[{"value":"420.8 kB"}],"format":"application/pdf","licensetype":"license_11","mimetype":"application/pdf","url":{"label":"SC-PR-OHASHI-R-kaken 2014-4p.pdf","url":"https://kanazawa-u.repo.nii.ac.jp/record/45618/files/SC-PR-OHASHI-R-kaken 2014-4p.pdf"},"version_id":"dc1888b5-3aa1-4c1a-ae6c-fa4f6239672c"}]},"item_language":{"attribute_name":"言語","attribute_value_mlt":[{"subitem_language":"jpn"}]},"item_resource_type":{"attribute_name":"資源タイプ","attribute_value_mlt":[{"resourcetype":"research report","resourceuri":"http://purl.org/coar/resource_type/c_18ws"}]},"item_title":"固体NMRによる結晶化が困難なタンパク質のための構造解析法の開発","item_titles":{"attribute_name":"タイトル","attribute_value_mlt":[{"subitem_title":"固体NMRによる結晶化が困難なタンパク質のための構造解析法の開発"},{"subitem_title":"Development of the structure analytical method for protein having difficulty in crystallization by the solid-state NMR","subitem_title_language":"en"}]},"item_type_id":"9","owner":"18","path":["2820"],"pubdate":{"attribute_name":"公開日","attribute_value":"2018-08-23"},"publish_date":"2018-08-23","publish_status":"0","recid":"45618","relation_version_is_last":true,"title":["固体NMRによる結晶化が困難なタンパク質のための構造解析法の開発"],"weko_creator_id":"18","weko_shared_id":-1},"updated":"2023-07-27T09:17:55.665937+00:00"}