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Quantitative analysis of major elements in igneous rocks with X-ray fluorescence spectrometer “ZSX primus II” using a 1:10 dilution glass bead
https://doi.org/10.24517/00011111
https://doi.org/10.24517/000111112225bea5-d179-489e-9da8-5f712d58834c
名前 / ファイル | ライセンス | アクション |
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AA00835991-31-44-KUSANO.pdf (624.7 kB)
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Item type | 紀要論文 / Departmental Bulletin Paper(1) | |||||
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公開日 | 2017-10-03 | |||||
タイトル | ||||||
タイトル | Quantitative analysis of major elements in igneous rocks with X-ray fluorescence spectrometer “ZSX primus II” using a 1:10 dilution glass bead | |||||
言語 | ||||||
言語 | eng | |||||
キーワード | ||||||
主題Scheme | Other | |||||
主題 | Quantitative analysis | |||||
キーワード | ||||||
主題Scheme | Other | |||||
主題 | Major element | |||||
キーワード | ||||||
主題Scheme | Other | |||||
主題 | X-ray fluorescence spectrometer(XRF) | |||||
キーワード | ||||||
主題Scheme | Other | |||||
主題 | ZSX primus II | |||||
キーワード | ||||||
主題Scheme | Other | |||||
主題 | 1:10dilution glass beads | |||||
資源タイプ | ||||||
資源タイプ識別子 | http://purl.org/coar/resource_type/c_6501 | |||||
資源タイプ | departmental bulletin paper | |||||
ID登録 | ||||||
ID登録 | 10.24517/00011111 | |||||
ID登録タイプ | JaLC | |||||
著者 |
Kusano, Yuki
× Kusano, Yuki× Umino, Susumu× Kobayashi, Jinya× Mizukami, Tomoyuki× Okuno, Masayuki× Arai, Shoji |
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著者別表示 |
海野, 進
× 海野, 進× 水上, 知行× 奥野, 正幸× 荒井, 章司 |
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書誌情報 |
The science reports of the Kanazawa University = 金沢大学理科報告 巻 58, p. 31-44, 発行日 2014-01-01 |
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ISSN | ||||||
収録物識別子タイプ | ISSN | |||||
収録物識別子 | 0022-8338 | |||||
NCID | ||||||
収録物識別子タイプ | NCID | |||||
収録物識別子 | AA00835991 | |||||
出版者 | ||||||
出版者 | Institute of Science and Engineering, Kanazawa University = 金沢大学 | |||||
抄録 | ||||||
内容記述タイプ | Abstract | |||||
内容記述 | Detailed procedures of sample processing including preparation of a 1: 10 dilution glass bead and evaluations of calibration lines of the X-ray fluorescence spectrometer for major element compositions of igneous rock samples are presented. We used 11 igneous rock standard samples of the Geological Survey of Japan and the synthetic material for the calibration. A powdered rock sample ignited at 900 ° C for four hours and lithium tetraborate as an alkali flux ignited at 700 ° C for four hours are weighed 0.4000 ± 0.0001 g and 4.0000 ± 0.0001 g, respectively. The mixture of rock powder sample and lithium tetraborate is put into a platinum crucible and fused to a glass bead. The calibration lines for basalts and andesites named "Major12" analyze 10 major elements such as Si, Ti, Al, Fe, Mn, Mg, Ca, Na, K and P in 10 minutes. The result of repeated analyses of six standard materials shows that the relative standard deviations are less than 3% and relative errors are less than 1.2%. Therefore, the calibration lines "Major12" are sufficient to be applied to routine measurement of igneous rocks. For analysis of ultramafic rocks, another set of calibration lines "majorOl'' was made based on standard samples including synthesized materials of SiO, and MgO reagents, and the calibration lines cover wider Si, Mg, Ni and Cr ranges than "Major12". The calibration lines "majorOl'' successfully reproduced concentrations of nine major element compositions (Si, Ti, Al, Fe, Mn, Mg, Ca, Ni, Cr) of the standard samples of ultramafic rocks. | |||||
著者版フラグ | ||||||
出版タイプ | VoR | |||||
出版タイプResource | http://purl.org/coar/version/c_970fb48d4fbd8a85 |