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ニッケル内標法を用いた生体試料中白金の原子吸光分析
http://hdl.handle.net/2297/45660
http://hdl.handle.net/2297/456606cb55da4-67e3-49f1-966b-1641f12789b1
名前 / ファイル | ライセンス | アクション |
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Item type | 学術雑誌論文 / Journal Article(1) | |||||
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公開日 | 2017-10-04 | |||||
タイトル | ||||||
タイトル | ニッケル内標法を用いた生体試料中白金の原子吸光分析 | |||||
タイトル | ||||||
タイトル | Atomic Absorption Spectrophotometric Determination of Platinum in Biological Materials Using Nickel as an Internal Standard | |||||
言語 | en | |||||
言語 | ||||||
言語 | jpn | |||||
資源タイプ | ||||||
資源タイプ識別子 | http://purl.org/coar/resource_type/c_6501 | |||||
資源タイプ | journal article | |||||
著者 |
木津, 良一
× 木津, 良一× 濱木, 路子× 下沢, 充子× 宮崎, 元一 |
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書誌情報 |
臨床化学 = Japanese Journal of Clinical Chemistry 巻 13, 号 3, p. 155-160, 発行日 1984-01-01 |
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ISSN | ||||||
収録物識別子タイプ | ISSN | |||||
収録物識別子 | 0370-5633 | |||||
NCID | ||||||
収録物識別子タイプ | NCID | |||||
収録物識別子 | AN00252758 | |||||
DOI | ||||||
関連タイプ | isIdenticalTo | |||||
識別子タイプ | DOI | |||||
関連識別子 | 10.14921/jscc1971b.13.3_155 | |||||
出版者 | ||||||
出版者 | 日本臨床化学会 = Japan Society of Clinical Chemistry | |||||
抄録 | ||||||
内容記述タイプ | Abstract | |||||
内容記述 | A method for the determination of platinum in biological materials by using nickel as an internal standard was established.Ten μg of nickel was added to samples which contained platinum.Nickel spiked sample was digested with nitric acid and hydrogen peroxide. Acid digest was evaporated to dryness and the residue was dissolved in 0.5ml of IM nitric acid. The amount of platinum was measured byflameless atomic absorption spectrophotometer using background correction with deuterium Iamp, Nickel was measured by flame atomic absorption spectrophotometer. The amount of platinum measured was corrected by the amount of nickel measured.Limit of detection of platinum in the proposed method was 0.05 ppm and the calibration curve showed good linearity in the range from 0.1 to 2.0 ppm. The method is advantageous in reducing sample size and making highly sensitive analysis of p-atinum possible.Correction for the loss of p-atinum resulted from bumping or pretreatment of sample is also easy.The method will be helpful in determining platinum in pharmacological and pharmacokinetic studies of various antineoplastic platinum complexes. | |||||
権利 | ||||||
権利情報 | Copyright © Japan Society of Clinical Chemistry 日本臨床化学会 | |||||
権利URI | ||||||
権利情報 | https://www.jstage.jst.go.jp/browse/jscc1971b/-char/ja/ | |||||
著者版フラグ | ||||||
出版タイプ | VoR | |||||
出版タイプResource | http://purl.org/coar/version/c_970fb48d4fbd8a85 | |||||
関連URI | ||||||
識別子タイプ | URI | |||||
関連識別子 | http://www.jscc-jp.gr.jp/ | |||||
関連URI | ||||||
識別子タイプ | URI | |||||
関連識別子 | https://www.jstage.jst.go.jp/browse/jscc1971b/-char/ja/ |