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蛍光検出HPLCを用いるタバコ煙粒子中多環芳香族炭化水素の定量
http://hdl.handle.net/2297/44506
http://hdl.handle.net/2297/4450623c4c425-98e9-4d39-ba96-69a3cdcad6ef
| 名前 / ファイル | ライセンス | アクション |
|---|---|---|
PH-PR-TORIBA-A-23.pdf (862.9 kB)
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| Item type | 学術雑誌論文 / Journal Article(1) | |||||
|---|---|---|---|---|---|---|
| 公開日 | 2017-10-04 | |||||
| タイトル | ||||||
| タイトル | 蛍光検出HPLCを用いるタバコ煙粒子中多環芳香族炭化水素の定量 | |||||
| タイトル | ||||||
| タイトル | Quantification of Polycyclic Aromatic Hydrocarbons (PAHs) in Cigarette Smoke Particulates by HPLC with Fluorescence Detection | |||||
| 言語 | en | |||||
| 言語 | ||||||
| 言語 | jpn | |||||
| 資源タイプ | ||||||
| 資源タイプ識別子 | http://purl.org/coar/resource_type/c_6501 | |||||
| 資源タイプ | journal article | |||||
| 著者 |
鳥羽, 陽
× 鳥羽, 陽× 本間, 千春× 宇於崎, 和香× Chuesaard, Thanyarat× 唐, 寧× 早川, 和一 |
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| 書誌情報 |
分析化学 = Japan analyst 巻 63, 号 1, p. 23-29, 発行日 2014-01-01 |
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| ISSN | ||||||
| 収録物識別子タイプ | ISSN | |||||
| 収録物識別子 | 0525-1931 | |||||
| NCID | ||||||
| 収録物識別子タイプ | NCID | |||||
| 収録物識別子 | AA11681958 | |||||
| DOI | ||||||
| 関連タイプ | isIdenticalTo | |||||
| 識別子タイプ | DOI | |||||
| 関連識別子 | 10.2116/bunsekikagaku.63.23 | |||||
| 出版者 | ||||||
| 出版者 | 日本分析化学会 = The Japan Society for Analytical Chemistry | |||||
| 抄録 | ||||||
| 内容記述タイプ | Abstract | |||||
| 内容記述 | A high-performance liquid chromatographic (HPLC) method with fluorescence detection was developed for the quantification of polycyclic aromatic hydrocarbons (PAHs) in cigarette mainstream and sidestream smoke particulates. Fifteen kinds of PAHs classified as priority pollutants by the US EPA were quantified with six perdeuterated PAHs as internal standards. The smoke filter samples obtained from 3 brands of cigarettes using standardized smoking conditions were extracted with dichloromethane, and then treated with tandem solid phase extraction cartridges (Silica and Neutral Alumina). The limits of detection ranged from 0.24 to 2.2 pg, and were more sensitive than those by GC-MS. The analytes were quantified by using the internal standards, and the developed method achieved sufficient reproducibility and accuracy. The PAH levels in mainstream and sidestream smoke from 3 cigarette brands were in the range of 0.2 – 305 ng cigarette−1 and 26.4 – 6160 ng cigarette−1, respectively. The total PAH content in sidestream smoke was more than 10 times higher compared with that of mainstream smoke. This method should be useful as an optional analytical method to quantify PAHs in cigarette smoke particulates. | |||||
| 権利 | ||||||
| 権利情報 | Copyright © The Japan Society for Analytical Chemistry | |||||
| 著者版フラグ | ||||||
| 出版タイプ | VoR | |||||
| 出版タイプResource | http://purl.org/coar/version/c_970fb48d4fbd8a85 | |||||
| 関連URI | ||||||
| 識別子タイプ | URI | |||||
| 関連識別子 | https://www.jstage.jst.go.jp/browse/bunsekikagaku/-char/ja/ | |||||
| 関連URI | ||||||
| 識別子タイプ | URI | |||||
| 関連識別子 | http://www.jsac.jp/ | |||||
