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Crystal Structure of 4-Dimethylaminoazobenzene-4′-sulfonyl-L-tryptophan Dimethylsulfoxide Solvate
http://hdl.handle.net/2297/28469
http://hdl.handle.net/2297/2846910796688-3b81-4cd5-bf26-aedfb5fdb16f
| 名前 / ファイル | ライセンス | アクション |
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TE-PR-KUNIMOTO-K-117.pdf (82.5 kB)
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| Item type | 学術雑誌論文 / Journal Article(1) | |||||
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| 公開日 | 2017-10-03 | |||||
| タイトル | ||||||
| タイトル | Crystal Structure of 4-Dimethylaminoazobenzene-4′-sulfonyl-L-tryptophan Dimethylsulfoxide Solvate | |||||
| 言語 | ||||||
| 言語 | eng | |||||
| 資源タイプ | ||||||
| 資源タイプ識別子 | http://purl.org/coar/resource_type/c_6501 | |||||
| 資源タイプ | journal article | |||||
| 著者 |
Sasaki, Chizuru
× Sasaki, Chizuru× Kitoh, Soh-ichi× Hayashi, Hiroshige× Kunimoto, Koki |
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| 書誌情報 |
Analytical Sciences: X-ray Structure Analysis Online 巻 20, p. x117-x118, 発行日 2004-01-01 |
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| ISSN | ||||||
| 収録物識別子タイプ | ISSN | |||||
| 収録物識別子 | 1348-2238 | |||||
| DOI | ||||||
| 関連タイプ | isIdenticalTo | |||||
| 識別子タイプ | DOI | |||||
| 関連識別子 | 10.2116/analscix.20.x117 | |||||
| 出版者 | ||||||
| 出版者 | 日本分析化学会 = The Japan Society for Analytical Chemistry | |||||
| 抄録 | ||||||
| 内容記述タイプ | Abstract | |||||
| 内容記述 | Crystals of 4-dimethylaminoazobenzene-4′-sulfonyl-L-tryptophan dimethylsulfoxide solvate (Dabs-Trp·DMSO) are monoclinic, space group P21 with a = 12.941(6)Å, b = 7.760(3)Å, c = 14.131(7)Å, β = 103.161(8)° and Z = 2. The structure was solved by direct methods (SIR88) and refined to a final R value of 0.058 for 3152 reflections (I > 2.00σ(I)). The molecular geometries and conformations are comparable to the typical values of azobenzene and L-tryptophan. The DMSO molecule is involved in the intermolecular hydrogen bonds with the sulfonamide NH and the carboxyl OH groups of different Dabs-Trp molecules. The hydrogen-bonded chains propagate along the b axis, and are constructed from molecules related by a two-fold screw axis. The sulfonamide S=O and the carboxyl C=O groups do not participate in hydrogen bonding. | |||||
| 権利 | ||||||
| 権利情報 | Copyright (c) 2005 by The Japan Society for Analytical Chemistry | |||||
| 著者版フラグ | ||||||
| 出版タイプ | VoR | |||||
| 出版タイプResource | http://purl.org/coar/version/c_970fb48d4fbd8a85 | |||||
| 関連URI | ||||||
| 識別子タイプ | URI | |||||
| 関連識別子 | http://wwwsoc.nii.ac.jp/jsac/ | |||||
| 関連URI | ||||||
| 識別子タイプ | URI | |||||
| 関連識別子 | https://japanlinkcenter.org/JST.JSTAGE/analscix/20.x117 | |||||
